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This is a well-balanced, thorough, and clearly written introduction to the subject. It features excellent illustrations and homework problems throughout, making it invaluable as a textbook. The book progresses in a logical and clear fashion from the fundamentals through to advanced topics, such as disorder, twinning, microfocus sources, low energy electron diffraction, charge flipping, protein crystallography, the maximum likelihood method of refinement, and powder, neutron, and electron diffraction. The author's clear writing style and distinctive approach is well suited for chemists,...

This volume of Inorganic Syntheses spans the preparations of wide range of important inorganic, organometallic and solid-state compounds. The volume is divided into 6 chapters. The first chapter contains the syntheses of
some key early transition metal halide clusters and the very useful mononuclear molybdenum(III) synthon, MoCl₃(THF)₃. Chapter 2 covers the synthesis of a number of cyclopentadienyl compounds, including a novel route to sodium and potassium cyclopentadienide, MC₅H₅. Chapter 3 details synthetic procedures for a range of...