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The coordination chemistry of azo-heterocyclic compounds of silver (I), cadmium(II), manganese(II), ruthenium(0) and ruthenium(II) have been described. A newly designed unsymmetrical bi-heterocyclic azo compound, pyridyl-azo-imidazole has also been characterized in this book. The complexes have been characterized by microanalytical and spectroscopic data. Manganese(II) forms tetrahedral complex and has been characterized by their spectra, magnetic and electrochemistry. Pyridyl-azo-imidazoles form metallo-macrocyclic compound with silver(I) and with cadmium(II) a tetrahedral structure have...