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This comprehensive lab manual contains step-by-step protocols for orga nozinc compounds. It covers organozinc reagents using classical method s and using active zinc, modern electrolysis, and ultrasound. It also covers organic synthesis, including cyclopropanation reactions, transi tion-metal catalyzed reactions, and the use of organozinc reagents in asymmetric synthesis.

The second edition of Comprehensive Organic Synthesis--winner of the 2015 PROSE Award for Multivolume Reference/Science from the Association of American Publishers--builds upon the highly respected first edition in drawing together the new common themes that underlie the many disparate areas of organic chemistry. These themes support effective and efficient synthetic strategies, thus providing a comprehensive overview of this important discipline.

Fully revised and updated, this new set forms an essential reference work for all those seeking information on the solution of...

In recent years the choice of a given solvent for performing a reaction has become increasingly important. More and more, selective reagents are used for chemical transformations and the choice of the solvent may be determining for reaching high reaction rates and high selectivities. The toxicity and recycling considerations have also greatly influenced the nature of the solvents used for industrial reactions. Thus, the development of reactions in water is not only important on the laboratory scale but also for industrial applications. The p- formance of metal-catalyzed reactions in water for...