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Fly ash has been converted to zeolite using alkali fusion followed by hydrothermal treatment. The synthesis conditions were optimized to obtain highest conversion of fly ash to X-type zeolite. The prepared catalyst has demonstrated good efficiency in catalytic cracking of pure components, like n-Heptane, as well as heavy gas oil. The cracking activity of synthesized catalyst showed comparable activity with 13X zeolite and FCC catalyst collected from Bharat Petroleum Corporation Ltd., India. The activity of the synthesized catalyst has been tested for lkylation of phenol. The prepared ...