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In the present work electrochemical methods, namely "cyclic voltammetry" and "in-situ catalyst potential measurements", were applied for ex-situ and in-situ studies of catalysts respectively. Lactose oxidation was used as a model reaction. The combination of these two electrochemical methods gives a possibility for continuous characterization of metal containing heterogeneous catalysts during all steps of their life cycle - from synthesis to complete deactivation. The purpose of the ex-situ approach was to develop a common electrochemical method to characterize all VIII group metal catalysts....