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This book offers a systemic introduction and summarization of nanoscale characterization techniques on cementitious materials. Cementitious composites are ubiquitous in the realm of construction, serving as the backbone of infrastructure worldwide. These materials, typically composed of cement, aggregates, and water, exhibit a complex interplay of mechanical, chemical, and physical properties. In the introductory chapter, we delve into the fundamental aspects of cementitious composites, exploring their composition, structure, and significance in the construction industry. In the second...