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This book highlights crucial parameters and strategies in photocatalytic water splitting. The process utilizes light energy to drive the separation of water into hydrogen and oxygen with the help of a photocatalyst. The efficiency and performance of catalytic activities are determined by various parameters supported by material characterizations. Commonly, the catalytic performances in visible-light photocatalytic water splitting are governed by bandgap energy, surface area, crystal structure, charge carrier dynamics, catalyst loading, cocatalyst, pH of solution, and reaction temperatures....