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The free-radical retrograde-precipitation polymerization (FRRPP) process was introduced by the author in the early 1990s as a chain polymerization method, whereby phase separation is occurring while reactive sites are above the lower cr- ical solution temperature (LCST). It was evident that certain regions of the product polymer attain temperatures above the average ?uid temperature, sometimes rea- ing carbonization temperatures. During the early stages of polymerization-induced phase separation, nanoscale polymer domains were also found to be persistent in the reacting system, in apparent...

This monograph is a follow-up material to the first FRPPP book by Gerard Caneba in 2009. It includes additional conceptual results, implementation of the FRRPP process in emulsion media to produce various block copolymers, and other FRRPP-related supplementary topics. Conceptual topics include the application of the quantitative analysis presented in the first FRRPP monograph for the occurrence of the FRRPP process to the polysterene-styrene-ether (PS-S-Ether) and poly(methacrylic acid)-methacrylic acid-water (PMAA-MAA-Water) systems, as well as extensions through unsteady state analysis of...

This monograph is a follow-up to the first FRPPP book by Gerard Caneba. It includes additional conceptual results, implementation of the FRRPP process in emulsion media to produce various block copolymers, and other FRRPP-related supplementary topics.