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Breast and cervical cancers are the most common type of cancer among the female population of the Western world and is the leading cause of death in women. This disease can be cure if detected as early as possible. In Chapter 1, of the various conventional techniques in use, a brief discussion on how a healthy cervical tissue progresses into a cancerous one is discussed. Chapter 2 gives the description of Instrumentation involved in the photoluminescence spectroscopy and also the measurement of Polarized Emission of Fluorescence. Chapter 3 gives the theoretical background on Fluorescence...