This book is primarily meant to assist secondary school students offering Chemistry subject. It also acts as a good foundation to those offering this subject at advanced level. Chemistry is one of the most enjoyable subjects that any student can easily study and understand; it's enjoyable and passable. It has simple techniques some of which are covered in this book, and if you can master them, this subject will instead become an enjoyable game that you will always want to practice at home or during your free time. This book is divided into four sections including General Laboratory Guidelines and procedures that are normally ignored in a number of secondary schools, Volumetric Analysis, and Qualitative Analysis. You will find these techniques very easy to understand and enjoyable. Sections on inorganic qualitative analysis contain theoretical principles and experimental data explained in details with a number of examples to help a student. Both sections of qualitative and volumetric analysis expose some methods of treatment of experimental data. At the end of this book, a comprehensive appendix has been added for the practicing scientist.