Russian Contributions to Analytical Chemistry

ISBN-13: 9783319987903 / Angielski / Twarda / 2018 / 160 str.

Yury A. Zolotov

Opis

This book offers a unique perspective and novel information on the significant contributions of Russian scientists to analytical chemistry and chemical analysis.

Recenzje

"It provides an outstanding overview of the achievements in analytical science in Russia during the last century, when much of the development remained unrecognized outside the Soviet block. This book might be considered as a reference book for those interested in history of science, in particular analytical science of the twentieth century until now. ... the book is a unique resource to any scientist interested in the development of this field." (Reiner Salzer, Analytical and Bioanalytical Chemistry, Vol. 411, 2019)

Spis treści

Chapter 1. Spectroscopical methods

1.1. General remarks

1.2. Electrothermal atomic absorption spectrometry

1.3. Fluorescence analysis

1.4. Enhanced two-jet arc plasmatron and other works on atomic emission analysis

1.5. X-ray polycapillary optics

1.6. X-ray radiometric analysis and its applications

1.7. Other spectroscopical methods

References for Chapter 1

Chapter 2. Mass spectrometry and related methods

2.1. General remarks

2.2. Mass reflectron

2.3. Orthogonal entry of a continuous ion beam

2.4. Orbitrap: orbital ion trap

2.5. Electrospray ionization (ERIAD technique)

2.6. Ion-molecular reactions as a path to chemical ionization

2.7. Secondary ion mass spectrometry and fast atom bombardment

2.8. Atmospheric pressure photoionization

2.9. Resonance electron capture negative ion mass spectrometry

2.10. In pursuit of ultra-high resolution

2.11. Ion mobility increment spectrometry

References for Chapter 2

Chapter 3. Chromatographic methods

3.1. General remarks

3.2. Birth of chromatography

3.3. Thin-layer chromatography

3.4. Development of gas chromatography

3.5. Liquid–gas chromatography and chromato-membrane methods

3.6. Enantioselective ligand-exchange chromatography

3.7. Critical chromatography of polymers

3.8. Polycapillary and monolithic chromatographic columns

3.9. Countercurrent chromatography in inorganic analysis

3.10. Other works on chromatography

References for Chapter 3

Chapter 4. Electrochemical methods

4.1. General remarks

4.2. Ion-selective electrodes and electronic tongue

4.3. Voltammetry, especially its stripping version

4.4. Other achievements in the area of electrochemical methods

References for Chapter 4

Chapter 5. Chemical methods of analysis

5.1. General remarks

5.2. Some chemical reactions

5.3. Determination of elements using organic reagents

5.4. Development of titrimetric methods

5.5. Kinetic methods

5.6. Other chemical methods

References for Chapter 5

Chapter 6. Separation and preconcentration methods (apart from chromatography)

6.1. General remarks

6.2. Methodology of analytical preconcentration

6.3. Liquid–liquid extraction

6.4. New sorbents and their application to preconcentration

6.5. Capillary isotachophoresis and other separation techniques

References for Chapter 6

Chapter 7. Other methods

7.1. General remarks

7.2. Stoichiographic method of differentiating dissolution

7.3. Method of molecular condensation nuclei

7.4. Express tests methods

7.5. Elucidation of the structure of organic compounds using spectroscopical data

7.6. Semiconductor gas sensors

7.7. Some original novel devices and appliances

References for Chapter 7

Chapter 8. Analysis of specific objects. Analytical chemistry of individual analytes and

their groups

8.1. General remarks

8.2. Nuclear materials

8.3. Materials for microelectronics and other high-purity substances

8.4. Rare elements, platinum-group metals

8.5. Environmental objects

8.6. Other analysis objects and analytes

8.7. Ensuring the quality of chemical analysis

References for Chapter 8

Chapter 9. Textbooks. Journals. History and methodology of analytical chemistry.

Promotion of this science

9.1. General remarks

9.2. Textbooks and handbooks. Serial publications

9.3. Journals

9.4. Works on the history and methodology of analytical chemistry

9.5. Promotion and popularization of analytical chemistry

References for Chapter 9

Chapter 10. Organizational input

10.1. General remarks

10.2. Work in international organizations

10.3. Work in international journals

10.4. Organization of international conferences

10.5. Russian researchers abroad

10.6. Experience of organizing research in Russia

References for Chapter 10

O autorze

Yury A. Zolotov is the Head of the Department of Analytical Chemistry at Lomonosov Moscow State University, Russian Federation. He is the Editor-in-Chief of the Journal of Analytical Chemistry and the author of several books in Russian, English, German, Japanese and Romanian.

Blurb

This book offers a unique perspective and novel information on the significant contributions of Russian scientists to analytical chemistry and chemical analysis. Written by the Editor-in-Chief of the Journal of Analytical Chemistry, it discusses various examples of new methods and approaches originating in Russia, such as chromatography, electrothermal atomic absorption spectrometry, Kumakhov X-ray optics, the Spolský effect in fluorescent analysis and important innovations in mass spectrometry, which are already widely used. Other original developments, such as the chromatomembrane and stoichiographic methods, are on their way to international recognition. Tremendous expertise in the analysis of minerals and high-purity and special-purpose substances has accumulated in Russian laboratories, and as such this book appeals to anyone interested in the development of science in Russia; to physicists, chemists, and other specialists dealing with chemical analysis; and to postgraduates and students of chemistry-related disciplines.