Organic Syntheses, Collective Volume 9

ISBN-13: 9780471242482 / Angielski / Twarda / 1998 / 864 str.

Jeremiah P. Freeman; Richard Freeman

Opis

Reflecting the increased pace of research and the many recent advances in organic chemistry, this series serves as a single-source compendium of the most up-to-date and significant procedures currently in use. Volume 9 consists of checked procedures previously published in annual volumes, revised and updated.

Spis treści

Partial table of contents:

Synthesis of 2–Substituted Naphthalenediol Derivatives Using Chromium Carbene Complexes: 1–Acetoxy–2–Butyl–4–Methoxynaphthalene.

Highly Reactive Calcium for the Preparation of Organocalcium Reagents: Preparation of 1–Adamantylcalcium Halides and Their Addition to Ketones: 1–(1–Adamantyl) Cycohexanol.

Bis(Trifluoroethyl)(Carboethoxymethyl)Phosphonate.

N–tert––Butoxycarbonyl–2–Bromopyrrole.

Allylic Alcohols by Alkene Transfer from Zirconium to Zinc: 1–[(tert–Butyldiphenylsilyl)Oxy]–Dec–3–En–5–Ol.

1,3,5–Cyclooctatriene.

Diethyl 1–Propyl–2–Oxoethylphosphonate.

3, 4–Diethylpyrrole.

Dialkyl Mesoxalates by Ozonolysis of Dialkyl Benzalmalonates: Dimethyl Mesoxalate.

Manganese–Copper–Catalyzed Conjugate Addition of Organomagnesium Reagents to ,beta–Ethylenic Ketones: 2–(1,1–Dimethylpentyl)–5–Methyl Cyclohexanone.

4–Dodecylbenzenesulfonyl Azides.

Ethyl 2–Methyl–5–Phenyl–3–Furancarboxylate.

Preparation and Reactions of Alkenylchromium Reagents: 2–Hexyl–5–Phenyl–1–Penten–3–OL.

Preparation and Use of (Methoxymethoxy)Methyllithium: 1–(Hydroxymethyl) Cycloheptanol.

Acetylenic Ethers from Alcohols and Their Reduction to Z– and E–Enol Ethers: 1–Menthoxy–1–Butyne.

Methyl 5–Methoxyindole–2–Acetate.

A General Method for the Preparation of –Branched Amino Acids: (S)–2–Methyl Proline.

Synthesis of Epoxides Using Dimethyldioxirane: trans–Stilbene Oxide.

Tris(Trimethylsilyl)Silane.

Indexes.