Inductively Coupled Plasma Emission Spectroscopy, Part 1: Methodology, Instrumentation and Performance

ISBN-13: 9780471096863 / Angielski / Twarda / 1987 / 608 str.

Inductively Coupled Plasma Emi; P. W. Boumans; P. W. J. M. Boumans

Opis

In the 1960s, the development of inductively coupled plasmas (ICP) as excitation sources for atomic emission spectroscopy (AES) permitted, for the first time, the convenient, simultaneous determination of a number of chemical elements in solutions. In two self-contained volumes, this is the first definitive text/reference on ICP-AES since the introduction of this important analytical technique. Part 1 of Inductively Coupled Plasma Emission Spectroscopy covers the basis of ICP-AES as an analytical method and discusses fundamental analytical concepts, performance, and figures of merit; principles of the instrumentation; the relation between ICP and other modern "plasma sources;" and the connection between ICP-AES, on one hand, and ICP atomic fluorescence spectroscopy and ICP mass spectroscopy, on the other. Part 2 examines applications and fundamentals of the technique. The overall treatment of the subject is tutorial, systematic, and consistent. The approach is scientific and rigorous, but mathematical formulae are used only when they promote clarity. Aside from filling a void in the AES literature, Inductively Coupled Plasma Emission Spectroscopy provides a critical survey of more than 20 years of research, development, and application in the field of ICP and related plasma sources. It is an excellent handbook for both novices and experts, and it serves as an aidememoire and major source of reference for analytical spectroscopists, analytical chemists, physical chemists and physicists, including those who are researchers, technicians, and applied analysts.

Spis treści

Introduction to Atomic Emission Spectrometry.

Plasma Sources other than Inductively Coupled Plasmas.

Inductively Coupled Plasmas.

Basic Concepts and Characteristics of ICP–AES.

Torches for Inductively Coupled Plasmas.

Sample Introduction Techniques in ICP–AES.

Line Selection and Spectral Interferences.

Spectrometers.

Detection and Measurement.

Index.

O autorze

About the editor P. W. J. M. Boumans, Chief Scientist with Philips Research Laboratories in Eindhoven, The Netherlands, has conducted research at the forefront of atomic spectroscopy for more than 25 years. He has published the now–classical book, Theory of Spectrochemical Excitation, and many important articles on ICP optimization, detection limits, line selection, and spectral interferences, including a two–volume tabulation, "Line Coincidence Tables for ICP Atomic Emission Spectrometry." In 1979, he became Editor–in–Chief of the journal, Spectrochimica Acta, Part B, Atomic Spectroscopy, after serving as editor seven years. He also serves on the editorial boards of Progress in Analytical Spectroscopy, The ICP Information Newsletter, Analusis, and Talanta. Dr. Boumans studied chemistry and physics at the University of Amsterdam, where he obtained his doctor′s degree cum laude in 1961.

Blurb

Tandem Mass Spectrometry Edited by F. W. McLafferty More than 50 contributors, representing 32 of the world’s leading research groups in mass spectrometry, examine the fundamentals, methods, instrumentation and applications of MS/MS, as well as promising new directions. The book describes the general types of MS/MS applications, primarily trace analysis in complex mixture, molecular structure elucidation, and gaseous ion reaction mechanisms; basic methods and theory, including the production and dissociation of characteristic ions; the principal types of instruments employed; special techniques; and applications of MS/MS in numerous fields. 506 pp. (0 471–86597–4) 1983 Molecular Luminescence Spectroscopy Methods and Applications, Part One Edited by Stephen G. Schulman Providing encyclopedic coverage, the author examines the applications of fluorescence, phosphorescence, and chemiluminescence spectra to the analysis of organic and inorganic compounds. The book features discussions of topics never presented in an analytical text, such as excited state optical activity and bioinorganic luminescence spectroscopy, and exhaustive reviews of fluorescence and phosphorescence of pharmaceuticals. Chapters on fluorescence detection in chromatography and luminescence immunoassay are the most up–to–date treatments available on these subjects. 826 pp. (0 471–86848–5) 1985 Auger Electron Spectroscopy M. Thompson, M. Baker, A. Christie, and J. Tyson After comparing AES with other techniques in the general field of electron spectroscopy, this book reviews the fundamentals and theories underlying the AES effect. The authors experienced users of AES offer an easy–to–follow summary of procedures along with generic descriptions of equipment components. The book also deals with a sequence of studies of gas phase spectra from rare gases to metals to molecules. Chemical aspects of the methods are discussed, followed by a particularly comprehensive description of AES with reference to materials science. 375 pp. (0 471–04377–X) 1985