In-Situ Transmission Electron Microscopy Experiments: Design and Practice

ISBN-13: 9783527347988 / Angielski / Twarda / 2023 / 400 str.

Khalid Hattar; Renu Sharma

Spis treści

IN-SITU TEMGeneral Scope of the Book and Review of the ChaptersWhy in-situ TEM?TEM OverviewTEM/STEM-Based Characterization TechniquesOther TechniquesIntroduction to Different Stimuli Used for In situ TEMEXPERIMENT DESIGN PHILOSOPHYGeneral AspectsChoice of Technique and the MicroscopeTEM Holder Design and SelectionSpecimen Design and PreparationGuidelines for Experimental SetupPractical Example of Designing In-situ TEM ExperimentsApplications to Quantitative DataIN-SITU HEATINGHistoryCurrently Available Heating HoldersExperimental ConsiderationsSelect ApplicationsLimiations and PossibilitiesIN SITU CRYO-TEMHistorical PerspectiveSpecimen Holder Design and FunctionSpecimen Design and PreparationPractical Aspects of Performing Cryogenic CoolingSome Noteworthy ApplicationsDESIGNING LIQUID AND GAS CELL HOLDERSHistorical PerspectiveDesign PhilosophyWindowsMicrofabricated Window-Cell (Microchips)Examples of Modified Window HoldersIN SITU SOLID-LIQUID INTERACTIONSHistorical PerspectiveHolder Design and SelectionSpecimen Design and PreparationData AcquisitionPractical ChallengesSelect Examples of ApplicationsIN-SITU GAS-SOLID INTERACTIONSHistorical PerspectiveCurrent StrategiesGas Manifold Design and ConstructionPractical Aspects of Performi Experiment in Gas EnvironmentsSelect Examples of ApplicationsReview of Benefits and LimitationsMULTIMODAL AND CORRELATIVE MICROSCOPYMultimodal TEMCorrelative ApproachesDATA PROCESSING AND MACHINE LEARNINGHistory of Image Simulation and ProcessingCurrent StatusData ManagementData Processing and Machine Learning (ML)Select ApplicationsFuture NeedsLimitationsFUTURE VISIONHistorical AspectsCurrent StatusTechnical ChallengesDeveloping Relevant Strategies

O autorze

Renu Sharma received a B.S. and B.Ed. in Physics and Chemistry from Panjab University, India, and M.S. and Ph.D. degrees in Solid State Chemistry from the University of Stockholm, Sweden. She is currently a NIST Emeritus Fellow after working there as a project leader from 2009 to 2019. She came to NIST from Arizona State University (ASU), where she began as a Faculty Research Associate in the Department of Chemistry and Biochemistry and the Center for Solid State Science, served as a Senior Research Scientist in the LeRoy Eyring Center for Solid State Science and as an affiliated faculty member of the School of Materials and Department of Chemical Engineering. Dr. Sharma is one of the pioneers in the development of environment cell scanning/transmission electron microscopy (E(S)TEM), combining atomic-scale resolution with dynamic chemical analysis of gas-solid reactions. She has applied this powerful technique to characterize atomic-scale mechanisms underlying the synthesis and reactivity of nanoparticles (including catalysts), nanotubes, nanowires, inorganic solids, ceramics, semiconductors, and superconductor materials. She has over 180 publications to her name.