Kategoria BISAC: Science >> Chemistry - Organic

In a single volume, Monosaccharide Sugars critically summarizes the applied and potentially useful strategies for the synthesis and degradation of monosaccharides by chain-elongation, degradation, and epimerization. These methodologies permit the synthesis of rare or unnatural monosaccharides that are frequently employed as chiral building blocks in natural products synthesis, as well as for producing sugar derivatives labeled with radioactive isotopes. Representative and well-established experimental procedures are provided to illustrate the potential of the synthetic...

In the case of students, this laboratory preparations manual can be used to find additional experiments to illustrate concepts in synthesis and to augment existing laboratory texts. A name reaction index is also included to direct the reader to the location where specific reactions appear in this manual.

The industrial chemist is frequently required to prepare a variety of compounds, and this manual can serve as a convenient guide to choose a synthetic route.

• Offers detailed directions for the synthesis of various functional groups
• Includes up-to-date...

This revised and updated second edition of Polymer Syntheses, Volume I brings together useful preparative methods for polymers and resins by functional group type that are of interest to both academic and industrial researchers. Several new directions for polymerization procedures have been included and are organized by various methodologies. Tables of physical property data and preparations make this book a valuable addition to any research library or research group.

• Provides detailed directions for the synthesis of various functional groups
• Includes up-to-date...

This revised and updated Second Edition of Polymer Synthesis II continues in the tradition of Volume I in presenting detailed laboratory instructions for the preparation of various polymers. Each chapter is organized by functional groups, and each chapter not only presents preparative methods, but also includes a brief introductory summary, reviews of the very latest journal articles and patents, and safety hazards and precautions. Procedures have been chosen on the basis of safety considerations and ease of being carried out with standard laboratory equipment. This comprehensive...

This volume, which completes the Second Edition of this widely respected three-volume set, continues the tradition of providing detailed and concise laboratory instructions for the preparation of organic and inorganic polymers. Updates are provided on the preparation of various types of polymers including olefin-sulfur dioxide copolymers, polythioesters, sulfide polymers, polyisocyanates, polyoxyalkylhydroxy compounds, polyvinyl carbazole, polyvinyl acetate, polyallyl esters, and polyvinyl flouride. The procedures were chosen on the basis of safety and to be representative of preparation...

Volume II describes 17 additional functional groups and presents a critical review of their available methods of synthesis with preparative examples of each. Attention is especially paid to presenting specific laboratory directions for the many name reactions used in describing the synthesis of these functional groups.

• This volume covers synthetic methods for the generation of 17 functional groups; Unique features include the citation of U.S. and foreign patent literature and safety information; Major topics discussed: Ynamines, Enamines, Allenes, Azo compounds, Azoxy compounds,...

This volume provides organic chemists with a convenient, up-to-date reference source on reliable preparative procedures for the most common functional groups. Preparations for each functional group have been subdivided into various reaction types.

The features of this book which will be of special interest to academic organic chemists are the introduction (Chapter 1), which presents a short course on the concepts and language of heterogeneous catalysis, covers organic reaction mechanisms of hydrogenation (Chapter 2), hydrogenolysis (Chapter 4), and oxidation (Chapter 6), a presents problems and solutions specific for running heterogeneous catalytic organic reactions in solution. These materials can supplement advanced chemistry courses.

Most synthetic organic chemists use a variety of "protecting groups" which they attach to...

This book describes the fascinating chemistry of the many kinds of organic compounds of hypervalent iodine. Each chapter deals with a particular iodine compound or families of compounds which have been used as reagents in a plethora of useful transformations. These include assorted oxidation, such as with the precious Dess-Martin reagent as well as with a wide range of further reactions.

Prominent features of hypervalent iodine reagents derived from iodobenzene are: ready availability, operational simplicity, mild reaction conditions, and high efficiency. They are environmentally...

The Handbook of Organic Compounds: NIR, IR, Raman, and UV-Vis Spectra Featuring Polymers and Surfactants represents a compendium of practical spectroscopic methodology, comprehensive reviews, and basic information for organic materials, surfactants, and polymer spectra covering the Ultraviolet, Visible, Near Infrared, Infrared, Raman and Dielectric measurement techniques. This set represents a complementary organic compound handbook to the Nyquist inorganic handbook, published in 1996. This set comprises the first comprehensive multi-volume handbook to provide basic coverage for...

The quantitative and informational characteristics of today's biomedical sciences have evolved so rapidly that students and scientists will increasingly use computers for calculation, sequence analyses, model-building, and testing hypotheses. The computer age has required biomedical workers to learn the steps involved in solving biomolecular calculations and to understand the theoretical basis of experimental procedures. This text does more than provide a catalog of biochemical calculations; in addition to showing how to perform certain calculations, it emphasizes mastery of basic theoretical...

Rubber elasticity is an important sub-field of polymer science. This book is in many ways a sequel to the authors' previous, more introductory book, Rubberlike Elasticity: A Molecular Primer (Wiley-Interscience, 1988), and will in some respects replace the now classic book by L.R.G. Treloar, The Physics of Rubber Elasticity (Oxford, 1975). The present book has much in common with its predecessor, in particular its strong emphasis on molecular concepts and theories. Similarly, only equilibrium properties are covered in any detail. Though this book treats much of the same...

This book aims to provide a succinct yet rigorous presentation of orga nic chemistry for readers with some background in the subject. The fir st five chapters review the basic principles of organic reactions and reactivity, such as structure and bonding, oxidation level, acidity an d basicity, curved arrow notation, stereochemistry, and conformation. Functional group manipulation is covered in the next chapter, while ch apters 7 and 8 concentrate on the methods employed in the production o f new carbon-carbon bonds. Practical concerns--the planning of organic syntheses, the factors...

Molecular Orbital Calculations for Biological Systems is a hands-on guide to computational quantum chemistry and its applications in organic chemistry, biochemistry, and molecular biology. With improvements in software, molecular modeling techniques are now becoming widely available; they are increasingly used to complement experimental results, saving significant amounts of lab time. Common applications include pharmaceutical research and development; for example, ab initio and semi-empirical methods are playing important roles in peptide investigations and in drug design. The...

Polymer Chemistry is an introductory textbook intended for graduate and advanced undergraduate students and industrial chemists who work with polymers. The author's purpose in writing the book was to provide a comprehensive and up-to-date overview of the chemistry of macromolecular substances, with particular emphasis on polymers that are important commercially, and the properties that make them important. Major topics include polymer synthesis nomenclature, molecular weight, reactions of polymers, recycling of polymers, methods used for characterizing and testing polymers, morphology,...

This book is a synthesis of two of Hudlicky's earlier books outlining the many unpredictable properties of fluorine and its compounds that are not analogous to the properties of any other halogens and their compounds. It is divided into two separate sections, the first presenting peculiar reactions as problems to be solved. Each reaction can be analyzed in the lab without the help of the second section, however if a solution is not easily reached, the second section provides discussion of the problems, outlining the products of the reactions and their mechanisms. Among the 105 reactions...

Searching for reaction in organic synthesis has been made much easier in the current age of computer databases. However, the dilemma now is which procedure one selects among the ocean of choices. Especially for novices in the laboratory, it becomes a daunting task to decide what reaction conditions to experiment with first in order to have the best chance of success. This collection intends to serve as an "older and wiser lab-mate" one could have by compiling many of the most commonly used experimental procedures in organic synthesis. With chapters that cover such topics as functional group...

Searching for reaction in organic synthesis has been made much easier in the current age of computer databases. However, the dilemma now is which procedure one selects among the ocean of choices. Especially for novices in the laboratory, it becomes a daunting task to decide what reaction conditions to experiment with first in order to have the best chance of success. This collection intends to serve as an "older and wiser lab-mate" one could have by compiling many of the most commonly used experimental procedures in organic synthesis. With chapters that cover such topics as functional group...

This comprehensive lab manual contains step-by-step protocols for orga nozinc compounds. It covers organozinc reagents using classical method s and using active zinc, modern electrolysis, and ultrasound. It also covers organic synthesis, including cyclopropanation reactions, transi tion-metal catalyzed reactions, and the use of organozinc reagents in asymmetric synthesis.

Samir Zard provides a description of radical reactions and their applications in organic synthesis. This book shows that an with an elementary knowledge of kinetic and some common sense, it is possible to harness radicals into a tremendously powerful tool for solving synthetic problems.