This book provides information on characterizing the microstructure and mechanical properties of cementitious materials at microscale. Specifically, with the intention to  provide the methods of preparing the samples for the micro-scale mechanical testing, to address the techniques for measuring and analyzing the elastic modulus, the stiffness, and the fracture toughness of cementitious materials at micro scale by instrumented indentation, to describe a method for measuring and interpreting creep behavior of cementitious materials at micro scale, and to demonstrate the homogenization...