This textbook, supported by the Textbook Publishing Center of University of Chinese Academy of Sciences, provides a fundamental introduction to advanced diagnostics techniques for graduate students majoring in combustion science, chemistry, and chemical engineering-related subjects. The textbook provides an overview with respect to the spectroscopic methods in advanced diagnostics techniques such as gas chromatography/mass spectrometry, thermochemical analysis, Raman scattering, and nuclear magnetic resonance. It then describes the comprehensive basic theory, equipment structure, and testing...