The application of supercritical carbon dioxide has been attracting more attention in the synthesis of biodegradable polymers. Highly pure products without residues can be recovered after the polymerization in supercritical carbon dioxide. In this book, the synthesis steps of polyester-based biodegradable polymers and the production of nanofiber scoffolds from these polymers are reported in details. For the synthesis of polyester-based biodegradable polymers, three types of block fluorinated poly(L-lactide-co- -caprolactone) are synthesized in supercritical carbon dioxide using reactive...