Synthesis of Inorganic Materials

ISBN-13: 9783527310371 / Angielski / Miękka / 2005 / 429 str.

Ulrich Schubert; Nicola Husing

Opis

This second edition of a very well received advanced textbook retains the chemist's viewpoint in its comprehensive overview of methods for chemical synthesis of inorganic materials.

The second chapter now includes a section on biomorphic ceramics, while one on LEDs has been added to Chapter 3. Chapter 4 now includes a more thorough explanation of borate glasses, with certain sections being completely rearranged. In addition, Chapter 6 has been extensively revised, and a whole new sub-chapter added on coordination polymers.

The general principles and requirements are discussed for each method given, along with selected examples of technically applied materials, as well as the material properties and applications of the resulting products. Furthermore, numerous tables with further examples help in assessing the scope and limitation of the various methods and in choosing a suitable synthesis for any given problem.

Intended for both courses in inorganic chemistry and materials science, this volume is equally valuable for all researchers working on the borderline of these two disciplines.

Spis treści

INTRODUCTION
SOLID–STATE REACTIONS
Reactions Between Solid Compounds
Solid –Gas Reactions
Decomposition and Dehydration Reactions
Intercalation Reactions
Further Reading
FORMATION OF SOLIDS FROM THE GAS PHASE
Chemical Vapor Transport
Chemical Vapor Deposition
Aerosol Processes
Further Reading
FORMATION OF SOLIDS FROM SOLUTIONS AND MELTS
Glass
Precipitation
Biomaterials
Solvothermal Processes
Sol–Gel Processes
Further Reading
PREPARATION AND MODIFICATION OF INORGANIC POLYMERS
General Aspects
Polysiloxanes (Silicones)
Polyphosphazenes
Polysilanes
Polycarbosilanes
Polysilazanes and Polycarbosilazanes
Other Inorganic Polymers
Further Reading
POROUS MATERIALS
Introduction to Porosity
Metallic Foams and Porous Metals
Aerogels
Porous Solids with an Ordered Porosity
Incorporation of Functional Groups into Porous Materials
Further Reading
NANOSTRUCTURED MATERIALS
Nanoparticles and Nanocrystalline Materials
Nanotubes
Mono– and Multilayers
Further Reading
GLOSSARY
INDEX

O autorze

Ulrich Schubert is Professor of Inorganic Chemistry at the Institute of Materials Chemistry, Vienna University of Technology. Born in Regensburg, he completed all his studies at the Technical University of Munich, including his thesis under the supervision of E.O. Fischer. He was a post–doctoral fellow at Stanford University, where he worked with W.S. Johnson. After gaining his lecturing qualification in Munich, he held a professorship of inorganic chemistry at the University of Würzburg from 1982 to 1994 before moving to Vienna to become a full professor. From 1989 to 1994 he also served in different positions at the Fraunhofer Institute of Silicate Research in Würzburg. Professor Schubert′s research interests include application–oriented fundamental research on sol–gel processes and the activation of silicon–element bonds by transition metal complexes.

Nicola Hüsing is assistant professor at the Institute of Materials Chemistry at Vienna University of Technology. Born in Rheda–Wiedenbrück, she studied chemistry at the University of Würzburg. While working on her dissertation she began working at Vienna University of Technology and the University of California, Los Angeles. After receiving her PhD in 1997 from the University of Würzburg, she was awarded a post–doctoral fellowship with C.J. Brinker on nanostructured thin films the following year. Returning to Vienna she gained her lecturing qualification in 2003 and is taking up a full professorship at the University of Ulm this year. Her research interests focus on the synthesis of sol–gel based porous materials and mesoscopically organized systems, especially with respect to synthesis – structure – property relations.