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This book provides the preparation and deposition of Nickel, Cobalt and Copper nanoparticles on graphite substrate by using electroless plating method. The analytical techniques such as FESEM, XRD, EDX, ZPA, XPS, CV and EIS were used to confirm the deposition, composition, morphology and activity of the Ni/Co/Cu oxides on graphite substrate. The graphite surface was activated by the introduction of catalytic nuclei and deposited by immersion electroless plating. The method gives an efficient and cost-effective way for obtaining the graphite deposited with the nanoparticles of Nickel, Cobalt...