NMR Spectroscopy in Liquids and Solids

ISBN-13: 9781138406902 / Angielski / Twarda / 2017

Vladimir I. Bakhmutov

Opis

NMR Spectroscopy in Liquids and Solids provides an introduction of the general concepts behind Nuclear Magnetic Resonance (NMR) and its applications, including how to perform adequate NMR experiments and interpret data collected in liquids and solids to characterize molecule systems in terms of their structure and dynamics.The book is composed of ten chapters. The first three chapters consider the theoretical basis of NMR spectroscopy, the theory of NMR relaxation, and the practice of relaxation measurements. The middle chapters discuss the general aspects of molecular dynamics and their relationships to NMR, NMR spectroscopy and relaxation studies in solutions, and special issues related to NMR in solutions. The remaining chapters introduce general principles and strategies involved in solid-state NMR studies, provide examples of applications of relaxation for the determination of molecular dynamics in diamagnetic solids, and discuss special issues related to solid state NMR� including NMR relaxation in paramagnetic solids. All chapters are accompanied by references and recommended literature for further reading. Many practical examples of multinuclear NMR and relaxation experiments and their interpretations are also presented. The book is ideal for scientists new to NMR, students, and investigators working in the areas of chemistry, biochemistry, biology, pharmaceutical sciences, or materials science.

Recenzje

"…a valuable and comprehensive introduction to general concepts behind NMR spectroscopy and a condense overview illustrating the multiple facets of NMR applications in various analytical domains. …compared with the existing literature, this book proposes various insights on unusual NMR topics. From this aspect, it is therefore a worthwhile addition to any up-to-date NMR library."
—Philippe Lesot, in Analytical and Bioanalytical Chemistry

Spis treści

Physical Basis of Nuclear Magnetic Resonance. Chemical Shift and Nuclear Coupling. Nuclear Relaxation: Theory and Measurements. NMR and Molecular Dynamics: General Principles. NMR Spectroscopy in Solutions: Practice and Strategies of Structural Studies. NMR Relaxation in Solutions: Applications. Solution NMR: Special Issues. Solid-State NMR Spectroscopy: General Principles and Strategies. Molecular Dynamics and Nuclear Relaxation. Solid-State NMR: Special Issues. Concluding Remark.

O autorze

Vladimir I. Bakhmutov works in the Department of Chemistry at Texas A&M University in College Station. He earned his PhD in physical inorganic chemistry from Moscow State University. Dr. Bakhmutov's research interests include extensive applications of solution and solid state NMR techniques for chemistry, molecular physics, and materials science. Dr. Bakhmutov has been granted visiting professorships by Zurich University, Switzerland; Bourgogne University, Dijon, France; Rennes University, France; CINVESTAV, Mexico; and Iberdrola, Zaragosa, Spain. He is the author or co-author of more than 300 scientific articles and five books.