Fabrication of TiO2 Nanotubes Using Electrochemical Anodization » książka
Fabrication of TiO2 Nanotubes Using Electrochemical Anodization
ISBN-13: 9783659157721 / Angielski / Miękka / 2012 / 132 str.
In this work, describes the synthesis of self-organized titanium dioxide nanotube layers by an electrochemical anodization of Ti at different conditions (time, voltage, concentration of NH4F in electrolyte with glycerol, conductivity and water content) at room temperature ( 25 C) were investigated. In the current study, self-organized, vertically-oriented TiO2 nanotubes were successfully prepared by anodization method of a pure Titanium sheet (99.5%) using anodization cell is designed for first time in Iraq (Homemade) from Teflon material according to our knowledge to produce self-ordered Titanium nanotube in organic based electrolytes (glycerol based electrolyte) an electrolyte solution containing (0.5, 1, 1.5 and 2 wt.% NH4F) then added water (2 and 5Wt.% H2O) to (0.5wt.% NH4F) only with 15V. The range of anodizing time and potential were between 1-4hr. and 5-40V, where Wt.% represent weight percentage. Scanning electron microscopy (SEM), Atomic force microscopy (AFM) and (XRD) X-Ray diffraction were employed to characterize the morphology and structure of the obtained Titania templates, optical interferometer (Fizeau frings) method to tubes length measurement."
In this work, describes the synthesis of self-organized titanium dioxide nanotube layers by an electrochemical anodization of Ti at different conditions (time, voltage, concentration of NH4F in electrolyte with glycerol, conductivity and water content) at room temperature (~25ºC) were investigated. In the current study, self-organized,vertically-oriented TiO2 nanotubes were successfully prepared by anodization method of a pure Titanium sheet (99.5%) using anodization cell is designed for first time in Iraq (Homemade) from Teflon material according to our knowledge to produce self-ordered Titanium nanotube in organic based electrolytes (glycerol based electrolyte) an electrolyte solution containing (0.5, 1, 1.5 and 2 wt.% NH4F) then added water (2 and 5Wt.% H2O) to (0.5wt.% NH4F) only with 15V. The range of anodizing time and potential were between 1-4hr. and 5-40V, where Wt.% represent weight percentage. Scanning electron microscopy (SEM), Atomic force microscopy (AFM) and (XRD) X-Ray diffraction were employed to characterize the morphology and structure of the obtained Titania templates, optical interferometer (Fizeau frings) method to tubes length measurement.
Czytaj nas na:
KrainaKsiazek.PL - Księgarnia Internetowa
