Analytical Calorimetry: Volume 5

ISBN-13: 9781461296775 / Angielski / Miękka / 2011 / 402 str.

F. Julian;Philip S. Johnson;Gill

Opis

This Volume 5 in a continuing series represents the compilation of papers presented at the International Symposium on Analytical Calorimetry as part of the 185th National Meeting of the American Chemical Society, Seattle, Washington, March 20-25th. 1983. A much broader variety of topics are covered than in pre vious volumes, due to the growth in the field of Thermal Analysis. Specific topics covering such techniques as differential scanning calorimetry, combined thermogravimetric procedures, dynamic mechan ical analysis and a variety of novel kinetic analyses are covered. A wide range of material types are included in this volume such as polymers (alloys, blends and composites), fossil fuels, biological products, liquid crystals and inorganic materials. The co-editors of this volume would like to thank all the contributors for their efforts in conforming to the manuscript requirements, and for being prompt in the preparation. We would also like to thank those who presided over sessions during the course of the symposium; Professor Anselm C. Griffin, Professor Roger S. Porter and Dr. Edith A. Turi."

Spis treści

Coupling of DSC and Dynamic Mechanical Experiments for Probing Processing-Structure-Property Relationships of Catalyst Modified High Performance Epoxy Matrices.- On the Glass Transition of Polycrylamide.- The Binary Blends, Transreaction and Copolymers of Bisphenol-A Polycarbonate and a Polyarylate.- Curie Temperatures of the ICTA Certified Reference Materials.- Thermal Analysis of Acrylamide-Based Polymers.- Defining B-Stage and Total Cure for a Dicy Based Epoxy Resin by DSC.- Differential Scanning Calorimetry: Simultaneous Temperature and Calorimetric Calibration.- Dynamic Mechanical Analysis Application to Dynamic Thermomechanometry.- Applications of Differential Rheometry.- Materials Characterization Using Thermogravimetry Coupled to Triple Quadrupole Tandem Mass Spectrometry (MS/MS).- Calorimetric Response of Fossil Fuel Systems: Prospects and Problems.- Multiple Sample Differential Scanning Calorimetry.- Quantitative Evaluation of the Gibbs-DiMarzio Theory of the Glass Transition for Polystyrene.- Study on Adhesives Performance by Dynamic Mechanical Techniques.- Effect of Molecular Structure of Mesomorphism. 151. Thermal and X-ray Diffraction Analysis of a “Siamese Twin” Series: The 4,4’-Dicarboxy-?,?-Diphenoxyalkanes.- Reversibility and Capacity of Different Energy Storage Reactions by Calorimetry.- Power Scanning Calorimetry (PSC).- A Combined TG-GC-MS System for Materials Characterization.- A New Approach for Determining Mechanical Properties of Thermoset Resins.- The Melting Temperature of Polymers: Theoretical and Experimental.- Nonequilibrium Thermodynamics and Modern Dynamic Thermal Analysis Techniques.- Integral-Differential Relationships in Thermal Analysis.- The Characterization of Water in Treed Crosslinked Polyethylene Films.- Application of Combined Thermogravimetry Atmospheric Pressure Chemical Ionization Mass Spectrometry to Copolymer Analysis.- Semi-Automated Measurement of Composites Flexural Stress Relaxation.- Some Uses of Differential Scanning Calorimetry in Biomembrane Research.- The Effect of Sample Temperature Gradients on DSC Thermograms at the Glass Transition Temperature.- Characterization of Coal Liquefaction Residues by Thermal Methods of Analysis.- Computer Automation of the Dynamic Mechanical Analyzer and its Application to Cure Kinetics Studies and Dynamic Mechanical Property Analysis of Organic Coatings.- Cure Reaction Kinetics Characterization of Some Model Organic Coatings Systems by FT-IR and Thermal Mechanical Analysis.- Contributors.